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2022 – Marker Substances in the Aroma of Truffles

von

Ruben Epping¹, Lilly Bliesener¹, Dr. Tilman Weiss², Matthias Koch¹, *
¹Division of Organic Trace Analysis and Food Analysis, Bundesanstalt für Materialforschung und -Prüfung, Berlin, Germany
²sglux GmbH, Berlin, Germany
*Authors to whom correspondence should be addressed.

Marker Substances in the Aroma of Truffles

Abstract
The aim of this study was to identify specific truffle marker substances within the truffle aroma. The aroma profile of different truffle species was analyzed using static headspace sampling with gas chromatography mass spectrometry analysis (SHS/GC-MS). Possible marker substances were identified, taking the additional literature into account. The selected marker substances were tested in an experiment with 19 truffle dogs. The hypothesis “If trained truffle dogs recognize the substances as supposed truffles in the context of an experiment, they can be regarded as specific” was made. As it would be nearly impossible to investigate every other possible emitter of the same compounds to determine their specificity, this hypothesis was a reasonable approximation. We were interested in the question of what it is the dogs actually search for on a chemical level and whether we can link their ability to find truffles to one or more specific marker substances. The results of the dog experiment are not as unambiguous as could have been expected based on the SHS/GC-MS measurements. Presumably, the truffle aroma is mainly characterized and perceived by dogs by dimethyl sulfide and dimethyl disulfide. However, as dogs are living beings and not analytical instruments, it seems unavoidable that one must live with some degree of uncertainty regarding these results.

2021 – TOCONs with reduced dead times used for the detection of fire and combustion burner flames

von

Dr. Tilman Weiss, sglux GmbH, Berlin, Germany

TOCONs for the detection of fire and combustion burner flames

Abstract
The standard sglux TOCONs are featured by a relatively high time constant that extends from 30 ms (low sensitivity TOCONs) until 80 ms (high sensitivity TOCONs). Most of the TOCON applications benefit from this high time constant because usually the TOCON’s application is to measure a UV irradiation that slowly changes. Such applications are e.g. the control of UV disinfection and UV curing sources. Short changes of signal caused by electromagnetic or high frequency influences are averaged – which is a benefit. However, looking at flame detection in heaters or looking at fire detection applications this relatively high time constant may cause problems. The present report presents opportunities to reduce the dead time of the TOCONs.

2021 – Sensing ultraviolet light emission from hydrogen flames: Flame detection and flame monitoring in CO2 emission free domestic boilers

von

Bielefeld, S.E., TU Delft Electrical Engineering, Mathematics and Computer Science


Master Thesis

Abstract
As a contribution to the decarbonisation of domestic heating, the graduation project investigates the feasibility of the application of UV sensor technology for flame detection and flame monitoring in hydrogen-powered domestic gas boilers. The research includes empirical studies and an analytical approach to describe influences on the sensor signal strength.

2021 – How two sglux photodiodes contribute to the NASA 2021 Perseverance mission

von

Luther W. Beegle et al.
Space Sci Rev (2021) 217:58

Perseverance’s Scanning Habitable Environments with Raman and Luminescence for Organics and Chemicals (SHERLOC) Investigation

Abstract
The Scanning Habitable Environments with Raman and Luminescence for Organics and Chemicals (SHERLOC) is a robotic arm-mounted instrument on NASA’s Perseverance rover. SHERLOC has two primary boresights. The Spectroscopy boresight generates spatially resolved chemical maps using fluorescence and Raman spectroscopy coupled to microscopic images (10.1 μm/pixel). The second boresight is a Wide Angle Topographic Sensor for Operations and eNgineering (WATSON); a copy of the Mars Science Labora- tory (MSL) Mars Hand Lens Imager (MAHLI) that obtains color images from microscopic scales (∼13 μm/pixel) to infinity. SHERLOC Spectroscopy focuses a 40 μs pulsed deep UV neon-copper laser (248.6 nm), to a ∼100 μm spot on a target at a working distance of ∼48 mm. Fluorescence emissions from organics, and Raman scattered photons from organics and minerals, are spectrally resolved with a single diffractive grating spectrograph with a spectral range of 250 to ∼370 nm. Because the fluorescence and Raman regions are natu- rally separated with deep UV excitation (<250 nm), the Raman region ∼ 800 – 4000 cm−1 (250 to 273 nm) and the fluorescence region (274 to ∼370 nm) are acquired simultaneously without time gating or additional mechanisms. SHERLOC science begins by using an Aut- ofocus Context Imager (ACI) to obtain target focus and acquire 10.1 μm/pixel greyscale images. Chemical maps of organic and mineral signatures are acquired by the orchestration of an internal scanning mirror that moves the focused laser spot across discrete points on the target surface where spectra are captured on the spectrometer detector. ACI images and chemical maps (< 100 μm/mapping pixel) will enable the first Mars in situ view of the spa- tial distribution and interaction between organics, minerals, and chemicals important to the assessment of potential biogenicity (containing CHNOPS). Single robotic arm placement chemical maps can cover areas up to 7×7 mm in area and, with the < 10 min acquisition time per map, larger mosaics are possible with arm movements. This microscopic view of the organic geochemistry of a target at the Perseverance field site, when combined with the other instruments, such as Mastcam-Z, PIXL, and SuperCam, will enable unprecedented analysis of geological materials for both scientific research and determination of which sam- ples to collect and cache for Mars sample return.

2016-2021 – Investigation of UV-Aging behavior of components used in the production of UV-LEDs and UV-Sensors.

von

Partner: sglux GmbH
Research project within the 20zwanzig initiative «Advanced UV for life»
period: 2016 – 2021
acknowledgements: BMBF 03ZZ0123

Abstract
Within the UV-Aging project experimental setups and scientific method are developed to allow a reliable estimation of the degradation behavior of LED and photodiodes as well as components used in these products (glass, diffusors, reflectors, glues, etc.). In the beginning a UV-Aging chamber will be constructed which allows the control of UV light (UV-A, B & C), temperature (up to 170°C) and humidity (95% r.h.).

2020 – Inter-Comparison Campaign of Solar UVR Instruments under Clear Sky Conditions at Reunion Island (21°S, 55°E)

von

Jean-Maurice Cadet¹, Thierry Portafaix¹, Hassan Bencherif¹², Kévin Lamy¹, Colette Brogniez³, Frédérique Auriol³, Jean-Marc Metzger⁴, Louis-Etienne Boudreault⁵, Caradee Yael Wright⁶⁷
¹LACy, Laboratoire de l’Atmosphère et des Cyclones (UMR 8105 CNRS, Université de La Réunion, Météo-France), 97744 Saint-Denis de La Réunion, France.
²School of Chemistry and Physics, University of KwaZulu-Natal, Durban 4041, South Africa.
³Laboratoire d’Optique Atmosphérique, Université Lille, CNRS, UMR 8518, F-59000 Lille, France.
⁴Observatoire des Sciences de l’Univers de la Réunion, UMS 3365, 97744 Saint-Denis de la Réunion, France.
⁵Reuniwatt, 97490 Sainte Clotilde de la réunion, France.
⁶Department of Geography, Geo-informatics and Meteorology, University of Pretoria, Pretoria 0002, South Africa.
⁷Environment and Health Research Unit, South African Medical Research Council, Pretoria 0001, South Africa.

Int J Environ Res Public Health. 2020 Apr 21;17(8):2867. doi: 10.3390/ijerph17082867

Abstract
Measurement of solar ultraviolet radiation (UVR) is important for the assessment of potential beneficial and adverse impacts on the biosphere, plants, animals, and humans. Excess solar UVR exposure in humans is associated with skin carcinogenesis and immunosuppression. Several factors influence solar UVR at the Earth’s surface, such as latitude and cloud cover. Given the potential risks from solar UVR there is a need to measure solar UVR at different locations using effective instrumentation. Various instruments are available to measure solar UVR, but some are expensive and others are not portable, both restrictive variables for exposure assessments. Here, we compared solar UVR sensors commercialized at low or moderate cost to assess their performance and quality of measurements against a high-grade Bentham spectrometer. The inter-comparison campaign took place between March 2018 and February 2019 at Saint-Denis, La Réunion. Instruments evaluated included a Kipp&Zonen UVS-E-T radiometer, a Solar Light UV-Biometer, a SGLux UV-Cosine radiometer, and a Davis radiometer. Cloud fraction was considered using a SkyCamVision all-sky camera and the Tropospheric Ultraviolet Visible radiative transfer model was used to model clear-sky conditions. Overall, there was good reliability between the instruments over time, except for the Davis radiometer, which showed dependence on solar zenith angle. The Solar Light UV-Biometer and the Kipp&Zonen radiometer gave satisfactory results, while the low-cost SGLux radiometer performed better in clear sky conditions. Future studies should investigate temporal drift and stability over time.

2020 – UV sensors for hydrogen flame detection

von

Dr. Tilman Weiss, sglux GmbH, Berlin, Germany

UV sensors for hydrogen flame detection

Abstract
Pursuing the goal of decarburization of the energy use, the substition of petroleum gas by hydrogen gas produced with renewable energy is a very promising approach.

This requires a certain modification of the heaters. A major change will be the modification of the EN298 compliant flame sensing feature. Currently, sensing petroleum gas flames, electric ionization sensors are used – a rugged, reliable and inexpensive method. However, if hydrogen gas is added to the petroleum gas or if the gas entirely consists of hydrogen these ionization sensors can not be further applied. The reason is a changed reaction kinetics where the ionization effect can not be detected by these conventional sensors. This challenge can be mastered by use of opto-electronic UV sensors. These sensors reliably detect all kind of flames while “seeing” their characteristic emission spectrum in the ultraviolet light range. As UV sensors are more expensive than ionization detectors currently the UV sensors are only applied in highly priced industrial burners but not in household burners. However, according the current state of the knowledge, no other method than opto-electronic UV sensors are able to reliably detect a hydrogen flame.

Since 2006 we produce the TOCONs ABC1 and ABC2 for the EN298 compliant detection of petroleum gas flames in household burners. Our new TOCON_F series is designed for the detection of hydrogen flames.

The difference of the new TOCON_F to the standard ABC1 and ABC2 TOCONs is a reduced off dead-time. This off dead-time occurs with the standard TOCONs when they are saturated and can extend to several 100 milliseconds. The TOCON_F with its logarithmic amplifier shrinks this dead-time to less than 70 milliseconds. Accordingly the reaction time after the flame’s (unwanted) distinction could be strongly increased. Even if the standard TOCONs ABC1 and ABC2 are fast enough (compliant with EN298) to be applied in flame sensing modules (EN298 claims a reaction time of less than 1000 milliseconds) – the requirements of the EN298 standard could be tightened in the future. The reason of this assumption is the significantly higher rate of spread and ignition range of a hydrogen flame compared with a petroleum gas flame. Hence a UV sensor module that works with a TOCON_F offers shorter reaction times than currently required by the standard. This makes these flame sensing modules future-proof in case of a possible revision of the standard.

2020 – Temperature Coefficient of SiC UV Photodiodes

von

Stefan Langer, sglux GmbH, Berlin, Germany

SiC Temperature Coefficient

Abstract
This report assigns the temperature coefficient (TC) of sglux SiC-photodiodes in relation to the incident wavelength. It demonstrates that the temperature coefficient is slightly negative for incident wavelengths below 270nm. At appox. 270nm is it almost zero and then strongly rises towards positive values with increasing wavelengths. The report further explains the physical background of this phenomena.